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Additional Reading On Growing Ergot: Gulf Res. &#82&#101&#112&#46 &#51&#40&#49&#41&#44 &#112&#97&#103&#101&#115 &#49&#48&#53&#45&#49&#48&#57 (1970), "Observations &#111&#110&#13&#10&#67&#108&#97&#118&#105&#99&#101&#112&#115 &#112&#117&#114&#112&#117&#114&#101&#97 &#111&#110 &#83&#112&#97&#114&#116&#105&#110&#97 alterflora." Canadian Journal &#111&#102&#13&#10&#66&#111&#116&#97&#110&#121 &#86&#111&#108&#46 &#51&#53&#44 &#112&#97&#103&#101&#115 315-320 (1957), "Studies on Ergot in Gramineous Hosts.<br>" Pharmacognosy (1965), pages 321- 327. 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The mixture is allowed to stand at -20 C for about 1.5 hours during which the suspended material dissolves, and the d-lysergic acid is converted to the mixed anhydride of lysergic and trifluoroacetic acids. The mixed anhydride can be separated in the form of an oil by evaporating the solvent in vacuo at a temperature below 0 C, but this is not necessary. Everything must be kept anhydrous. Step II. Use Yellow light The solution of mixed anhydrides in acetonitrile from Step I is added to 150 ml of a second solution of acetonitrile containing 7.6 g of diethylamide. The mixture is held in the dark at room temperature for about 2 hours. The acetonitrile is evaporated in vacuo, leaving a residue of LSD-25 plus other impurities. The residue is dissolved in 150 ml of chloroform and 20 ml of ice water. The chloroform layer is removed and the aqueous layer is extracted with several portions of chloroform. The chloroform portions are combined and in turn washed with four 50 ml portions of ice-cold water. The chloroform solution is then dried over anhydrous Na2SO4 and evaporated in vacuo. Preparation #3 This procedure gives good yield and is very fast with little iso-lysergic acid being formed (its effect are mildly unpleasant). However, the stoichiometry must be exact or yields will drop. Step I. Use White light Sulphur trioxide is produced in anhydrous state by carefully decomposing anhydrous ferric sulphate at approximately 480 C. Store under anhydrous conditions. Step II. Use White light A carefully dried 22 litre RB flask fitted with an ice bath, condenser, dropping funnel and mechanical stirrer is charged with 10 to 11 litres of dimethylformamide (freshly distilled under reduced pressure). The condenser and dropping funnel are both protected against atmospheric moisture. 2 lb of sulphur trioxide (Sulfan B) are introduced drop wise, very cautiously stirring, during 4 to 5 hours. The temperature is kept at 0-5 C throughout the addition. After the addition is complete, the mixture is stirred for 1-2 hours until some separated, crystalline sulphur trioxide-dimethylformamide complex has dissolved. The reagent is transferred to an air- tight automatic pipette for convenient dispensing, and kept in the cold. Although the reagent, which is colourless, may change from yellow to red, its efficiency remains unimpaired for three to four months in cold storage. An aliquot is dissolved in water and titrated with standard NaOH to a phenolphthalein end point. Step III. Use Red light A solution of 7.15 g of d-lysergic acid mono hydrate (25 mmol) and 1.06 g of lithium hydroxide hydrate (25 mmol) in 200 ml of MeOH is prepared. The solvent is distilled on the steam bath under reduced pressure. the residue of glass-like lithium lysergate is dissolved in 400 ml of anhydrous dimethyl formamide. 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